H-1 NMR Spectrum of Acetanilide
The following chemical shifts were reported [1,2] for the protons of acetanilide:
| CH3 [1] |
2.1 |
 |
| para-H [1] |
7.0 |
| meta-H [1] |
7.2 |
| ortho-H [1] |
7.4 |
| NH [2] |
ca. 8.75 |
| [1] |
M. Hesse, H. Meier, B. Zeeh: Spektroskopische Methoden in der organischen Chemie,
Georg Thieme Verlag, Stuttgart, 2nd ed., 1984, p. 263. |
| [2] |
from a H-1 NMR spectrum shown by
Stephen Jones |
C-13 NMR Spectrum of Acetanilide
The following chemical shifts were reported [1] for the carbons of acetanilide:
| CH3 [1] |
24.1 |
 |
| para-C [1] |
124.1 |
| meta-C [1] |
128.7 |
| ortho-C [1] |
120.4 |
| ipso-C [1] |
138.2 |
| CO [1] |
169.5 |
| [1] |
M. Hesse, H. Meier, B. Zeeh: Spektroskopische Methoden in der organischen Chemie,
Georg Thieme Verlag, Stuttgart, 2nd ed., 1984, p. 263. |
| [2] |
there is a C-13 NMR spectrum shown by
Stephen Jones |
Acetanilide
 |
| Names |
IUPAC names
N-phenylacetamide
N-phenylethanamide
|
| Identifiers |
|
|
103-84-4  |
| ChEBI |
CHEBI:28884 |
| ChEMBL |
ChEMBL269644 |
| ChemSpider |
880 |
| EC number |
203-150-7 |
|
|
| Jmol-3D images |
Image |
| KEGG |
C07565 |
|
|
| UNII |
SP86R356CC |
| Properties[1][2] |
|
|
C8H9NO |
| Molar mass |
135.17 g·mol−1 |
| Odor |
Odorless |
| Density |
1.219 g/cm3 |
| Melting point |
114.3 °C (237.7 °F; 387.4 K) |
| Boiling point |
304 °C (579 °F; 577 K) |
|
|
<0.56 g/100 mL (25 °C) |
| Solubility |
Soluble in ethanol, diethyl ether, acetone, benzene |
| log P |
1.16 (23 °C) |
| Vapor pressure |
2 Pa (20 °C) |
| Hazards[3][4] |
| Safety data sheet |
External MSDS |
| GHS pictograms |
 |
| GHS signal word |
WARNING |
|
|
H302 |
|
|
P264, P270, P301+312, P330, P501 |
| Flash point |
174 °C (345 °F; 447 K) |
|
|
545 °C (1,013 °F; 818 K) |
Except where otherwise noted, data are given for materials in their standard state (at 25 °C [77 °F], 100 kPa).
|
 verify (what is:  / ?) |
| Infobox references |
|
|
Drying acetanilide
/////
No comments:
Post a Comment