GREEN ACETANILIDE SYNTHESIS AND SPECTRAL ANALYSIS

 



 

















 



 

H-1 NMR Spectrum of Acetanilide

The following chemical shifts were reported [1,2] for the protons of acetanilide:

CH3 [1]	2.1
para-H [1]	7.0
meta-H [1]	7.2
ortho-H [1]	7.4
NH [2]	ca. 8.75

[1]	M. Hesse, H. Meier, B. Zeeh: Spektroskopische Methoden in der organischen Chemie, Georg Thieme Verlag, Stuttgart, 2nd ed., 1984, p. 263.
[2]	from a H-1 NMR spectrum shown by Stephen Jones

C-13 NMR Spectrum of Acetanilide

The following chemical shifts were reported [1] for the carbons of acetanilide:

CH3 [1]	24.1
para-C [1]	124.1
meta-C [1]	128.7
ortho-C [1]	120.4
ipso-C [1]	138.2
CO [1]	169.5

[1]	M. Hesse, H. Meier, B. Zeeh: Spektroskopische Methoden in der organischen Chemie, Georg Thieme Verlag, Stuttgart, 2nd ed., 1984, p. 263.
[2]	there is a C-13 NMR spectrum shown by Stephen Jones

Acetanilide

Names
IUPAC names N-phenylacetamide N-phenylethanamide
Identifiers
CAS Registry Number	103-84-4
ChEBI	CHEBI:28884
ChEMBL	ChEMBL269644
ChemSpider	880
EC number	203-150-7
InChI[show]
Jmol-3D images	Image
KEGG	C07565
SMILES[show]
UNII	SP86R356CC
Properties[1][2]
Chemical formula	C8H9NO
Molar mass	135.17 g·mol−1
Odor	Odorless
Density	1.219 g/cm3
Melting point	114.3 °C (237.7 °F; 387.4 K)
Boiling point	304 °C (579 °F; 577 K)
Solubility in water	<0.56 g/100 mL (25 °C)
Solubility	Soluble in ethanol, diethyl ether, acetone, benzene
log P	1.16 (23 °C)
Vapor pressure	2 Pa (20 °C)
Hazards[3][4]
Safety data sheet	External MSDS
GHS pictograms
GHS signal word	WARNING
GHS hazard statements	H302
GHS precautionary statements	P264, P270, P301+312, P330, P501
Flash point	174 °C (345 °F; 447 K)
Autoignition temperature	545 °C (1,013 °F; 818 K)
Except where otherwise noted, data are given for materials in their standard state (at 25 °C [77 °F], 100 kPa).
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Infobox references

Drying acetanilide



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